Improved synthesis of 5 - allyloxy -2,3,4 - tris(benzyloxy)pentan -1 - ol
XI Zun-bo
LI Xin
MA Shu-tao
Abstract：Objective To synthesize 5 - allyloxy - 2,3,4 - tris(benzyloxy)pentan - 1 - ol. Methods With D - ri-bose as the starting material,5 - allyloxy - 2,3,4 - tris(benzyloxy)pentan - 1 - ol was obtained by glycosidation,benzyla-tion,hydrolyzation,oxime protection,allylation,deoximation and reduction. Results and Conclusion The overall yield of this method was 55% ,and the structure of product was characterized by 1H - NMR. The synthetic route was short and envi-ronmentally friendly,suitable for the industrial production.
Keywords：5 - Allyloxy - 234 - tris(benzyloxy)pentan - 1 - olSynthesisAntibodyRibose - ribitol
Publication Date：2015-01-01
Online Publishing Date：2025-08-15(First online date of this platform, not the publication date of the document)
Pages：3( 741-743 )