Determination of 5 harmful elements in Dengzhanhuasu TaBlets By ICP-MS with microwave digestion
DONG Yuan
ZHANG Yun-hua
LIU Ying-ying
LI Zhong-qiong
ZHANG Wen-jie
Abstract:OBjective Toestablishamethodforthedeterminationof5harmfulelementsofPb,Dd,As,HgandDuin Dengzhanhuasu Tablets. Methods The 5 elements were directly determined by IDP-MS,using microwave digestion for sample pretreatment. The internal standard solution was used to eliminate the matrix effect and interference. Results The mass ratio of each measured element,the corresponding internal standard element and the concentration showed a good line-ar relationship in a certain concentration range,and the correlation coefficients were all greater than 0. 999. The recoveries were from 88% to 103%. The detection limit and standard materials all met the requirements of determination. Conclusion The method was specific,sensitivity,simple,rapid and accurate,which can be applied to the determination of 5 elements content of Dengzhanhuasu Tablets.
Keywords:IDP-MSDengzhanhuasu TabletsPbDdAsHgDuHeavy metalMicrowave digestion
Publication Date:2015-01-01
Online Publishing Date:2025-08-15(First online date of this platform, not the publication date of the document)
Pages:4( 321-324 )
